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قابل دانلود از دوشنبه, ۲۳ مرداد ۱۴۰۲
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فهرست مطالب: Dedication ......... . vPreface ......... . . . . vii Contributors......... xiii 1 Introduction to Mass Spectrometry for Bimolecular Analysis in a Clinical Laboratory ........ . . . . 1 2 System Performance Monitoring in Clinical Liquid Chromatography-Tandem Mass Spectrometry (LC-MS/MS) .....13 3 Tandem Mass Spectrometry for the Analysis of Plasma/Serum Acylcarnitines for the Diagnosis of Certain Organic Acidurias and Fatty Acid Oxidation Disorders ........ . . . . . 27 4 Quantification of Plasma S-adenosylmethionine and S-adenosylhomocysteine Using Liquid Chromatography-Electrospray-Tandem Mass Spectrometry . . . . . 35 5 Quantitation of Aldosterone in Serum or Plasma Using Liquid Chromatography-Tandem Mass Spectrometry (LC-MS/MS) ..45 6 Comprehensive Determination of Amino Acids for Diagnosis of Inborn Errors of Metabolism ...... . 55 7 Quantification of Branched-Chain Amino Acids in Plasma by High-Performance Liquid Chromatography-Tandem Mass Spectrometry (LC-MS/MS) .....65 8 Quantitation of Butyrylcarnitine, Isobutyrylcarnitine, and Glutarylcarnitine in Urine Using Ultra-Performance Liquid Chromatography-Tandem Mass Spectrometry (UPLC-MS/MS) ..... . . . . 83 9 Quantification of Free and Total Carnitine in Serum Using Liquid Chromatography Tandem Mass Spectrometry .... . . . . . 95 10 Sensitive and Robust LC-MS/MS Analysis of Salivary Cortisol in Negative Mode....... . . . . . . 105 11 Measurement of Urinary Free Cortisol and Cortisone by LC-MS/MS .119 12 Laboratory Diagnosis of Cerebral Creatine Deficiency Syndromes by Determining Creatine and Guanidinoacetate in Plasma and Urine .. 129 13 Quantitation of Estradiol and Testosterone in Serum Using LC-MS/MS . . . . . . 141 14 Quantitation of Fatty Acids in Serum/Plasma and Red Blood Cells by Gas Chromatography-Negative Chemical Ionization-Mass Spectrometry........ . . 149 15 Quantitation of γ-Aminobutyric Acid in Cerebrospinal Fluid Using Liquid Chromatography-Electrospray-Tandem Mass Spectrometry........ . . 165 16 A Simple, Fast, and Reliable LC-MS/MS Method for the Measurement of Homovanillic Acid and Vanillylmandelic Acid in Urine Specimens .. . 175 17 Quantitation of Neuroblastoma Markers Homovanillic Acid (HVA) and Vanillylmandelic Acid (VMA) in Urine by Gas Chromatography–Mass Spectrometry (GC/MS) ....... 185 18 Quantification of 5-Hydroxyindoleacetic Acid in Urine by Ultra-performance Liquid Chromatography Tandem Mass Spectrometry ... . . . . . . 195 19 Quantitation of IgG Subclasses in Serum Using Liquid Chromatography–Tandem Mass Spectrometry (LC–MS/MS)..205 20 Quantification of Insulin Analogs by Liquid Chromatography–HighResolution Mass Spectrometry ...... . . 217 21 Differentiation of Common IGF-1 Variants Using HRMS COM Determination with Follow-Up MS/MS Verification...227 22 Monitoring and Identifying Insulin-Like Growth Factor 1 Variants by Liquid Chromatography–High-Resolution Mass Spectrometry in a Clinical Laboratory....... . 239 23 Quantitation of Lactate in Cerebrospinal Fluid Using Liquid Chromatography–Electrospray-Tandem Mass Spectrometry... . 253 24 Multiplex Lysosomal Enzyme Activity Assay on Dried Blood Spots Using Tandem Mass Spectrometry ..... . 261 25 Plasma Lysosphingolipid Biomarker Measurement by Liquid Chromatography Tandem Mass Spectrometry .... . . . . . 271 26 Detection of 13C-Mannitol and Other Saccharides Using Tandem Mass Spectrometry for Evaluation of Intestinal Permeability or Leaky Gut ........ . . 285 27 LC–MS/MS Method for High-Throughput Analysis of Methylmalonic Acid in Serum, Plasma, and Urine: Method for Analyzing Isomers Without Chromatographic Separation ..... . . . . 295 28 Quantitation of 5-Methyltetrahydrofolate in Cerebrospinal Fluid Using Liquid Chromatography-Electrospray-Tandem Mass Spectrometry........ . . 311 29 Screening of Organic Acidurias by Gas Chromatography–Mass Spectrometry (GC–MS) ....... 321 30 Identification of Urine Organic Acids for the Detection of Inborn Errors of Metabolism Using Urease and Gas Chromatography–Mass Spectrometry (GC/MS) ....... 335 31 Quantitative Organic Acids in Urine by Two-Dimensional Gas Chromatography-Time-of-Flight Mass Spectrometry (GCxGC-TOFMS)....... . . . . . 351 32 Quantification of Parathyroid Hormone and its Fragments in Serum by Liquid Chromatography–High-Resolution Mass Spectrometry .. . . . 365 33 High Sensitivity Measurement of Parathyroid Hormone–Related Protein (PTHrP) in Plasma by LC-MS/MS ....375 34 Quantitation of Phenylalanine in Dried Blood Spot Using Liquid Chromatography Tandem Mass Spectrometry for Monitoring of Patients with Phenylketonuria (PKU) ..... . . 391 35 An Optimized Procedure for Proteomic Analysis of Extracellular Vesicles Using In-Stage Tip Digestion and DIA LC-MS/MS: Application to Liquid Biopsy in Cancer..... . . . 401 36 High-Throughput Plasma Proteomic Profiling .... . . . . 411 37 Quantitation of Purine in Urine by Ultra-Performance Liquid Chromatography-Tandem Mass Spectrometry.... . . . . . 421 38 Quantitation of Pyrimidine in Urine by Ultra-Performance Liquid Chromatography-Tandem Mass Spectrometry.... . . . . . 431 39 Quantitation of Renin Activity in Plasma Using Liquid Chromatography-Tandem Mass Spectrometry (LC-MS/MS) ..439 40 Liquid Chromatography-Tandem Mass Spectrometry (LC-MS/MS) Method for the Quantification of Steroids Androstenedione, Dehydroepiandrosterone, 11-Deoxycortisol, 17-Hydroxyprogesterone, and Testosterone ....... . . . . . . 451 41 A User-Friendly Sample Preparation Alternative for Manual and Automated LC-MS/MS Quantification of Testosterone ... 459 42 Quantitation of Thyroglobulin in Serum Using SISCAPA and Liquid Chromatography-Tandem Mass Spectrometry (LC-MS/MS) ..473 43 Quantitation of Free Thyroxine by Equilibrium Dialysis and Liquid Chromatography-Tandem Mass Spectrometry.... . . . . . 485 44 Quantification of Tryptophan, Indole, and Indoxyl Sulfate in Urine Using Liquid Chromatography-Tandem Mass Spectrometry ... 493 45 Very-Long-Chain Fatty Acids Quantification by Gas-Chromatography Mass Spectrometry....... . . . . . 501 46 Quantification of Very-Long-Chain and Branched-Chain Fatty Acids in Plasma by Liquid Chromatography-Tandem Mass Spectrometry .. . . 509 47 High-Throughput Analysis of 25-OH-Vitamin D2 and D3 Using Multichannel Liquid Chromatography-Tandem Mass Spectrometry........ . . 523 48 Quantification of 25-Hydroxyvitamin D2 and D3 Using Liquid Chromatography-Tandem Mass Spectrometry.... . . . . . 539 Index ......... . . . . . 545 |
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فهرست به فارسی (ترجمه ماشینی): تقدیم ......... . v 25 اندازه گیری بیومارکر لیزوسفنگولیپید پلاسما توسط طیف سنجی جرمی پشت سر هم کروماتوگرافی مایع .... . . . . . 271 |
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مشخصات فایل |
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| عنوان (Title): | Applications of Mass Spectrometry in Biomolecular Analysis- Methods and Protocols |
| نام فایل (File name): | 1174-www.GeneProtocols.ir-Clinical Applications of Mass Spectrometry in Biomolecular Analysi.pdf |
| عنوان فارسی (Title in Persian): |
کاربردهای طیف سنجی جرمی در آنالیزهای بیومولکولی - روشها و پروتکل ها |
| ایجاد کننده: | Uttam Garg (editor) |
| زبان (Language): | انگلیسی English |
| سال انتشار: | 2022 |
| شابک ISBN: | 9781071625644 |
| نوع سند (Doc. type): | کتاب |
| فرمت (File extention): | |
| حجم فایل (File size): | 16.3 مگابایت |
| تعداد صفحات (Book length in pages): | 540 |
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